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NTEGRA platform: NTEGRA Spectra

  NTEGRA Spectra system has
won prestigious R&D 100 Award!
     
 
    Contact
Dr. Pavel Dorozhkin 

 
Confocal Raman/Fluorescence microscopy
Confocal Raman/Fluorescence/Rayleigh imaging runs simultaneously with AFM (during one sample scan)
Diffraction limited spatial resolution: <200 nm in XY, <500 nm in Z (with immersion objective)
True confocality; motorized confocal pinhole for optimal signal and confocality
Motorized variable beam expander/collimator: adjusts diameter and collimation of the laser beam individually for each laser and each objective used
Full 3D (XYZ) confocal imaging with powerful image analysis
Hyperspectral imaging (recording complete Raman spectrum in every point of 1D, 2D or 3D confocal scan) with further software analysis
Optical lithography (vector, raster)
AFM/STM: Integration with spectroscopy
Upright and Inverted optical AFM configurations (optimized for opaque and transparent samples correspondingly);
side illumination option
Highest possible resolution (numerical aperture) optics is used simultaneously with AFM: 0.7 NA for Upright, 1.3–1.4 NA for Inverted
AFM/STM and confocal Raman/Fluorescence images are obtained simultaneously (during one scan)
All standard SPM imaging modes are supported (>30 modes) — combined with confocal Raman/Fluorescence
Low noise AFM/STM (atomic resolution)
Vibrations and thermal drifts originating from optical microscope body are minimized due to special design of optical AFM heads
Focus track feature: sample always stays in focus due to AFM Z-feedback; high quality confocal images of very rough or inclined samples can be obtained
Software
Seamless integration of AFM and Raman; all AFM/ Raman/SNOM experiment and further data analysis is performed in one and the same software
Powerful analysis of 1D, 2D and 3D hyperspectral images 
Powerful export to other software (Excel, MatLab, Cytospec etc.)
Spectroscopy*
Extremely high efficiency 520 mm length spectrometer with 4 motorized gratings
Visible, UV and IR spectral ranges available
 
Echelle grating with ultrahigh dispersion; spectral resolution: 0.007 nm (< 0.1 1/cm)**
Up to 3 different detectors can be installed
  • TE cooled (down to -100 ºC) CCD camera. EMCCD camera is optional — for ultrafast imaging
  • Photon multiplier (PMT) or avalanche photodiode in photon counting mode
  • Photon multiplier for fast confocal laser (Rayleigh) imaging
Flexible motorized polarization optics in excitation and detection channels, cross-polarized Raman measurements 
Fully automated switch between different lasers — with a few mouse clicks
Scanning Near Field Optical Microscopy (SNOM)
Two major SNOM techniques supported: (i) based on quartz fiber probes, (ii) based on silicon cantilever probes
All modes supported: Transmission, Collection, Reflection 
All SNOM signals detected: laser intensity, fluorescence intensity, spectroscopy

SNOM lithography (vector, raster)

Optimized for Tip Enhanced Raman Scattering (TERS) and other tip-related optical techniques
(S-SNOM, TEFS, STM-LE etc.)
All existing TERS geometries are available: illumination/ collection from bottom, from top or from side
Different SPM techniques and TERS probes can be used: STM, AFM cantilever, quartz tuning fork in tapping and shear force modes
Dual scan (for Hot Point Mapping in TERS): scan by sample AND scan by tip / by laser spot
Motorized polarization optics to produce optimal polarization for TERS
 

AFM-Raman measurements can run in air, in controlled atmosphere or in liquid — all with variable temperature

Some features listed are optional — not included into basic system configuration
* NT-MDT AFM can be integrated with Renishaw inVia or with NT-MDT spectrometer. Specifications are given for the latter. Renishaw specifications can be found at www.renishaw.com/AFM-Raman
** Exact value of spectral resolution highly depends on how “resolution” is defined

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